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Gold carbonyl cations and beyond: homoleptic gold(I) complexes with P 4 and P 4 S 3 and the half-sandwich cation [Au(C 6 H 6 )(CO)] .
Chemical Communications : Chem Comm 2024 April 30
Oxidation of Au0 with the synergistic Ag+ /0.5 I2 system in the commercial organic solvent 1,2,3,4-tetrafluorobenzene led to the perfluoroalkoxyaluminate salt of the [Au(CO)2 ]+ cation known from superacid chemistry. This [Au(CO)2 ]+ salt proved to be an excellent 'naked' Au+ -synthon yielding complex salts with [Au(η2 -P4 )2 ]+ , [Au(η1 -P4 S3 )2 ]+ and half-sandwich [Au(η2 -C6 H6 )(CO)]+ cation.
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