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AlCl 3 -mediated ring-opening reactions of indoline-2-thiones with acyl cyclopropanes, bi-cyclopropanes and spirocyclic cyclopropanes.
Organic & Biomolecular Chemistry 2023 July 27
AlCl3 -mediated nucleophilic ring-opening reactions of indoline-2-thiones with various acyl cyclopropanes, bi-cyclopropanes and spirocyclic cyclopropanes were investigated. A series of ketones functionalized with indolylthio groups were synthesized in yields ranging from moderate to good. Moreover, chemical transformations of 4-indolylthio butan-1-ones to dihydro-2 H -thiepino[2,3- b ]indoles and sulfone were carried out to further expand both synthetic utility and structural complexity.
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