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Journal Article
Research Support, Non-U.S. Gov't
Total Synthesis of Neodysiherbaine A via 1,3-Dipolar Cycloaddition of a Chiral Nitrone Template.
Organic Letters 2017 December 2
The total synthesis of neodysiherbaine A was achieved via 1,3-dipolar cycloaddition of a chiral nitrone template with a sugar-derived allyl alcohol in the presence of MgBr2 ·OEt2 . This cycloaddition constructed the C2 and C4 asymmetric centers in a single step. Then reductive cleavage, intramolecular SN 2 reaction of the tertiary alcohol, and oxidation of the primary alcohol afforded neodysiherbaine A.
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