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Generation of cycloalkynes through deprotonation of cyclic enol triflates with magnesium bisamides.
Chemical Communications : Chem Comm 2017 Februrary 24
Deprotonative generation of cyclohexynes, cycloheptynes, and cyclooctynes was achieved by controlling the reactivities of transient anionic species from the corresponding enol triflates with magnesium bis(2,2,6,6-tetramethylpiperidide) as a base. The starting enol triflates are readily obtained through triflation of the corresponding ketones, allowing direct access to the cycloalkynes.
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