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Efficient Synthesis of 3-Mercaptoindoles via HI-Promoted Sulfenylation of Indoles with Sodium Sulfinates.

Shengnan Sun, Hexia Ye, Haibo Liu, Yongbiao Guo, Zhenhua Gao, Li Pan, Junchen Li, Xiaojing Bi
ChemistryOpen 2023 March
A new direct sulfenylation method of indoles by sodium sulfinates and hydroiodic acid was developed giving variety of 3-sulfenylindoles in high yields under mild conditions without using any catalysts or other additives. In situ-generated RS-I species are supposed to be mainly responsible for the key electrophilic alkyl- or aryl-thiolation process.

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