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Magnetic solid phase extraction of benzoylurea insecticides in tea samples with Fe 3 O 4 -hyperbranched polyester magnetic composite as sorbent.
Journal of Separation Science 2019 Februrary 16
In this work, a method for the analysis of benzoylurea insecticides, including hexaflumuron, flufenoxuron, lufenuron and chlorfluazuron, in tea samples by HPLC with Fe3 O4 - hyperbranched polyester nanocomposite as the adsorbent for magnetic solid-phase extraction was developed. The magnetic nanocomposite was prepared and characterized by infrared spectroscopy, vibrating sample magnetometry and scanning electron microscopy. The as-prepared nanocomposite was used as the sorbent for extraction and preconcentration of pesticide residues in tea samples. The extraction and desorption conditions, including mass ratios of raw materials, amount of sorbent, pH value, extraction time and desorption time, were investigated. Under the final conditions chosen for the analysis, good linearity was obtained for all the tested compounds, with R2 values of at least 0.9979. The limits of detection were determined in the range of 0.15-0.3 μg L-1 . The recovery obtained from the analysis of tea samples with various spiked concentrations was between 90.7% and 98.4%, with RSDs (n = 4) lower than 4.1%. Furthermore, the present approach was successfully applied to the quantitative determination of residues of benzoylurea insecticides in real samples. This article is protected by copyright. All rights reserved.
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