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Scalable Total Synthesis of (-)-Vinigrol.
Journal of the American Chemical Society 2019 Februrary 16
Vinigrol is a structurally and stereochemically complex natural product that displays various potent pharmacological activities, including the capability to modulate TNF-α. A new and efficient synthetic route towards this natural product has been developed to complete the asymmetric synthesis of (-)-vinigrol and provide over 600 mg material, manifesting the power of macrocyclic stereocontrol and transannular Diels-Alder reaction.
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