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1,4-Palladium Shift/C(sp 3 )-H Activation Strategy for the Remote Construction of Five-Membered Rings.
Organic Letters 2019 Februrary 9
1, n-Metal shift is an elegant alternative approach enabling the functionalization of remote C-H bonds from simple precursors. In this work, we report a novel and simple Pd0 -catalyzed domino reaction involving 1,4-palladium shift and C(sp3 )-H activation and leading to (fused) five-membered rings. This method allowed access to a broad range of valuable arylidene γ-lactams and indanones and was applied to the formal synthesis of (-)-pyrrolam.
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