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Estimation of filler macro-dispersion in rubber matrix by radiometric stereo microscopy.

Journal of Microscopy 2019 January 31
A new microscopic principle based on radiometric stereo microscopy is presented which is designed for investigating macro-dispersion of filler in rubber. The image acquisition is combined with a stereological method of estimating the volume-weighted size distribution of the filler particles. Experimental results for carbon black filler in rubber obtained by radiometric stereo microscopy are compared with those from microtomography using synchrotron radiation and, furthermore, a simulation study is used for evaluation. It turns out that using the new three-dimensional microscopic method, the size distribution of the filler particles can be estimated from fresh cuts of rubber with high accuracy, and thus it is an interesting alternative to well-established dark field microscopy. This article is protected by copyright. All rights reserved.

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