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Radical alkylation of isocyanides with amino acid-/peptide-derived Katritzky salts via photoredox catalysis.
Organic & Biomolecular Chemistry 2019 January 26
An efficient and mild method was developed for the synthesis of 6-alkylated phenanthridines upon visible light irradiation. Bench-stable and easily handled redox-active Katritzky pyridinium salts derived from abundant amino acids/peptides were used as radical precursors for the alkylation of isocyanobiphenyl species. The reaction displays an excellent functional group tolerance and a potential utility for peptide functionalization, allowing access to desired products in good to excellent yields.
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