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Pharmaceutico-analytical study of Samaguna , Dwiguna and Shadguna Balijarita Rasa Sindura .

Ayu 2018 January
Introduction: Rasa Sindura is a Kupipakva Rasayana which is very popular and is widely used in therapeutics till date. Therapeutic property of Rasa Sindura varies with proportion of Gandhaka added to Parada .

Aims and Objective: The present study was carried out to reevaluate and compare differences in the pharmaceutical analytical study of Rasa Sindura prepared with the changing proportion of Gandhaka . To prepare Samaguna (RS), Dwiguna (2RS) and Shadguna (6RS) Balijarita Rasa Sindura and to carry out X-ray diffraction study (XRD) and Fourier-Transform Infrared spectroscopy (FTIR) of the samples.

Material and Methods: Samaguna , Dwiguna and Shadguna Balijarita Rasa Sindura were prepared as per classical reference and the samples were subjected to XRD and FTIR.

Results: The duration of trituration for the preparation of Samaguna, Dwiguna and Shadguna Kajjali was 70, 40 and 24 h respectively. The duration of heating was 16, 16 and 19 h respectively. Average percentage yield of RS, 2RS and 6RS was 54%, 34.44% and 11.35%, respectively XRD showed increased crystallinity of the samples. FTIR spectrum revealed the decrease of unsaturated carbon and exchangeable proton as the proportion of sulfur increased in the preparation.

Conclusion: XRD and FTIR suggested better stability of the crystals of 6RS than 2RS and RS.

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