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Semireduction of Alkynes Using Formic Acid with Reusable Pd-Catalysts.

Riku Iwasaki, Eikichi Tanaka, Toshinari Ichihashi, Yasushi Idemoto, Kohei Endo
Journal of Organic Chemistry 2018 November 3
The treatment of PdCl2 with K2 CO3 and HCO2 H in dioxane gives black precipitates, which are an effective catalyst for the semireduction of alkynes to alkenes using formic acid as a reductant. Even 0.05 mol % Pd promoted the reduction reaction of tolane in high yield with high selectivity.

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