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Glassy carbon, NIST Standard Reference Material (SRM 3600): hydrogen content, neutron vibrational density of states and heat capacity.
Journal of Applied Crystallography 2018 October 2
Commercial glassy carbon plates being used as absolute intensity calibration standards in small-angle X-ray scattering applications (NIST SRM 3600) have been characterized in several recent publications. This contribution adds to the characterization by measuring the hydrogen content of a plate to be (4.8 ± 0.2) × 10-4 (mol H)/(mol C), and by measuring the vibrational spectrum by neutron inelastic scattering. The spectrum bears a strong resemblance to published measurements on graphite, allowing the identification of several spectral features. The measured spectrum is used to calculate the heat capacity of low-hydrogen-content glassy carbon for comparison with measurements reported here from 20 to 295 K.
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