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(Al,Mg) 3 La: a new phase in the Mg-Al-La system.
Acta Crystallographica Section B, Structural Science, Crystal Engineering and Materials 2018 August 2
During an investigation of the Mg-rich end of the Mg-Al-La system, a new ternary phase with the composition of (Al,Mg)3 La was identified. The crystal structure of this phase was determined by conventional X-ray powder diffraction and transmission electron microscopy analysis and refined using high-resolution X-ray powder diffraction. The (Al,Mg)3 La phase is found to have an orthorhombic structure with a space group of C2221 and lattice parameters of a = 4.3365 (1) Å, b = 18.8674 (4) Å and c = 4.4242 (1) Å, which is distinctly different from the binary Al3 La phase (P63 /mmc). The resolved structure of the (Al,Mg)3 La phase is further verified by high-angle annular dark-field scanning transmission electron microscopy.
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