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Arylation of Azaarylmethylamines with Aryl Chlorides and a NiBr 2 /NIXANTPHOS-based Catalyst.
Advanced Synthesis & Catalysis 2017 August 18
A nickel-catalyzed coupling of azaarylmethylamines with aryl chlorides has been achieved. NIXANTPHOS together with low cost NiBr2 was successfully developed and optimized to exhibit high reactivity at 2.5 mol % loading. Under optimized reaction conditions, aryl(azaaryl)methylamine products were afforded in good to excellent yields (22 examples, up to 98% yield).
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