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Journal Article
Research Support, Non-U.S. Gov't
Fluorous tagged N-hydroxy phthalimide for the parallel synthesis of O-aryloxyamines.
Journal of Combinatorial Chemistry 2010 September 14
The parallel synthesis of O-aryloxyamines remains an unfulfilled need in the field of medicinal chemistry and fragment-based approaches. To fill this gap a solution-phase two-step process based on (1) a copper-catalyzed cross-coupling of aryl boronic acids with a fluorous tagged N-hydroxyphthalimide, and (2) a supported aminolysis was designed and optimized using Taguchi's method. A library of O-aryloxyamines was synthesized in high yields with high purity and diversity.
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