Metrologia

A technique for characterizing and correcting the linearity of radiometric instruments is known by the names the "flux-addition method" and the "combinatorial technique". In this paper, we develop a rigorous uncertainty quantification method for use with this technique and illustrate its use with both synthetic data and experimental data from a "beam conjoiner" instrument. We present a probabilistic model that relates the instrument readout to a set of unknown fluxes via a set of polynomial coefficients. Maximum likelihood estimates (MLEs) of the unknown fluxes and polynomial coefficients are recommended, while a non-parametric bootstrap algorithm enables uncertainty quantification including standard errors and confidence intervals...

Constant-volume gas thermometry data published in 1989 for the difference between the thermodynamic temperature and the International Practical Temperature Scale of 1968 are corrected in two ways. A refined estimate of the thermal expansivity of the material of the gas bulb, published in 1990, increases the thermodynamic temperature by amounts on the order of 1 mK to 3 mK. Better knowledge of the nonideality of helium gas reduces the uncertainty of the nonideality correction to near zero and decreases the thermodynamic temperature by amounts on the order of 0...

Improvements in a lamp-monochromator-based facility at the National Institute of Standards and Technology (NIST), the Visible near-infrared Spectral Comparator Facility (VisSCF) which is used to calibrate optical detectors for spectral radiant power responsivity from 300 nm to 1100 nm, are described. These changes include extending the VisSCF operational range down to 300 nm from 350 nm, thereby fully covering the ultraviolet-A (UVA) spectral region and partially covering the UVB range. These improvements have lowered the magnitudes of most of the components in the uncertainty budget and have led to combined 0...

We demonstrate operation of a constant-pressure flowmeter capable of generating and accurately measuring flows as low as 2 × 10-13 mol/s. Generation of such small flows is accomplished by using a small conductance element with C ≈ 50 nL/s. Accurate measurement then requires both low outgassing materials (< 1 × 10-15 mol/s) and small volume changes (≈ 70 μ L). We outline the present flowmeter's construction, detail its operation, and quantify its uncertainty. The type-B uncertainty is < 0...

We have developed generalized methods for electrical substitution optical measurements, as well as cryogenic detectors which can be used to implement them. The new methods detailed here enable measurement of arbitrary periodic waveforms by an electrical substitution radiometer (ESR), which means that spectral and dynamic optical power can be absolutely calibrated directly by a primary standard detector. Cryogenic ESRs are not often used directly by researchers for optical calibrations due to their slow response times and cumbersome operation...

We show that the calibration of tri-axis accelerometers based on the device's intrinsic properties alleviates the uncertainty due to mounting misalignment in comparison to the use of the sensitivity matrix. The intrinsic properties of a tri-axis accelerometer are based on a ( u , v, w ) coordinate system that represent the direction of maximum sensitivities of each of the three accelerometers ( U, V, W ) and are assumed not to be perfectly orthogonal to each other. The calibration procedure requires rotation of the device in the gravitational field around each of the Cartesian coordinate ( x, y, z ) axes...

We use an array of transition-edge sensors, cryogenic microcalorimeters with 4 eV energy resolution, to measure L x-ray emission-line profiles of four elements of the lanthanide series: praseodymium, neodymium, terbium, and holmium. The spectrometer also surveys numerous x-ray standards in order to establish an absolute-energy calibration traceable to the international system of units for the energy range 4 keV to 10 keV. The new results include emission line profiles for 97 lines, each expressed as a sum of one or more Voigt functions; improved absolute energy uncertainty on 71 of these lines relative to existing reference data; a median uncertainty on the peak energy of 0...

We present the first measurements of kilowatt laser power with an uncertainty less than 1 %. These represent progress toward the most accurate measurements of laser power above 1 kW at 1070 nm wavelength and establish a more precise link between force metrology and laser power metrology. Radiation pressure, or photon momentum, is a relatively new method of non-destructively measuring laser power. We demonstrate how a multiple reflection optical system amplifies the pressure of a kilowatt class laser incoherently to improve the signal to noise ratio in a radiation pressure-based measurement...

No abstract text is available yet for this article.

NIST calibrates anemometers as a function of airspeed vector and turbulence intensity ( Tu ). The vector capability (sometimes called "3-D") is particularly important for calibrating multi-hole differential-pressure probes that are often used to quantify pollution emitted by smokestacks of coal-burning electric power plants. Starting with a conventional "1-D" wind tunnel, we achieved vector and Tu capabilities by installing translation/rotation stages and removable turbulence generators (grids or flags). The calibration ranges are: yaw angle ±180°; pitch angle ±45°; airspeed 1 m/s to 30 m/s; turbulence intensity 0...

Optical refractometry techniques enable realization of both pressure and temperature directly from properties of the gas. The NIST refractometer, a fixed length optical cavity (FLOC) has previously been evaluated for operation as pressure standard, and now in this paper, is evaluated for the feasibility of operation as a primary temperature standard as well. The challenge is that during operation, one cavity is filled with gas. Gas dynamics predicts that this will result in heating which in turn will affect the cavity temperature uniformity, impeding the ability to measure the gas temperature with sufficient accuracy to make the standard useful as a primary standard for temperature or pressure...

Despite ubiquitous implementation of the quartz crystal microbalance (QCM) for measuring thin film thickness throughout industry and academia, a direct link to the SI (International System of Units) does not exist. Confidence in QCM measurements relies on over a half-a-century of academic and industrial research used to understand the resonant frequency change due to loading mass onto a quartz crystal. Here, we use before and after gravimetric mass measurements, linked directly to the SI, to measure mass change...

Seven National Metrology Institutes (NMIs) from France, United States, United Kingdom, Russia, Mexico, China and Germany participated in an inter-laboratory comparison on thermal conductivity measurements by the Guarded Hot Plate method. This action was part of a series of supplementary inter-laboratory comparisons (including infrared spectral emittance and thermal diffusivity) sponsored by the Consultative Committee on Thermometry (CCT) Task Group on Thermophysical Quantities (TG-ThQ). The objective of this collaborative work was to strengthen the consistency of thermal conductivity measurements carried out worldwide on low conductive materials...

This paper presents a full characterization of a Dual Josephson Impedance Bridge (DJIB) at frequencies up to 80 kHz by using the DJIB to compare the best available impedance standards that are (a) directly traceable to the quantum Hall effect, (b) used as part of international impedance comparisons, or (c) believed to have calculable frequency dependence. The heart of the system is a dual Josephson Arbitrary Waveform Synthesizer (JAWS) source that offers unprecedented flexibility in high-precision impedance measurements...

The Monte Carlo method is an established tool that is often used to evaluate the uncertainty of measurements. For computationally challenging problems, Monte Carlo uncertainty analyses are typically distributed across multiple processes on a multi-node cluster or supercomputer. Additionally, results from previous uncertainty analyses are often used in further analyses in a sequential manner. To accurately capture the uncertainty of the output quantity of interest, Monte Carlo sample distributions must be treated consistently, using reproducible replicates, throughout the entire analysis...

We measure the detection efficiency of single-photon detectors at wavelengths near 851 nm and 1533.6 nm. We investigate the spatial uniformity of one free-space-coupled single-photon avalanche diode and present a comparison between fusion-spliced and connectorized fiber-coupled single-photon detectors. We find that our expanded relative uncertainty for a single measurement of the detection efficiency is as low as 0.70% for fiber-coupled measurements at 1533.6 nm and as high as 1.78% for our free-space characterization at 851...

The unique properties of the quantum Hall effect allow one to revisit traditional measurement circuits with a new flavour. In this paper we present the first realization of a quantum Hall Kelvin bridge for the calibration of standard resistors directly against the quantum Hall resistance. The bridge design is particularly simple and requires a minimal number of instruments. The implementation here proposed is based on the bridge-on-a-chip , an integrated circuit composed of three graphene quantum Hall elements and superconducting wiring...

Two-way satellite time and frequency transfer (TWSTFT) is a primary technique for the generation of coordinated universal time (UTC). At present, more than 12 timing laboratories around the world use SAtellite Time and Ranging Equipment (SATRE) modems in TWSTFT operations and contribute data for the realization of UTC. The advantages of TWSTFT are its small calibration uncertainty (≤1.0 ns if the link is calibrated with a TWSTFT mobile station) and its long-term link stability. However, the precision of SATRE TWSTFT in the operational networks is degraded by a daily variation pattern (diurnal) in the TWSTFT results...

No abstract text is available yet for this article.

Accurate determination of the bidirectional transmittance distribution function (BTDF) of transmissive diffusers is critical for the on-orbit spectral radiance calibration of several satellite-based, Earth remote sensing instruments. This study presents the results of the comparison of BTDF measurements by NASA Goddard Space Flight Center's Diffuser Calibration Laboratory and the National Institute of Standards and Technology's Spectral Tri-function Automated Reference Reflectometer facility on two transmissive diffusers: HOD-500, a synthetic fused silica sample manufactured by Hereaus Quarzglas and Spectralon-250, a sintered polytetrafluoroethylene sample manufactured by Labsphere, Incorporated...